[rescue] Oh my gosh, an on-topic question! ;^)
vance at neurotica.com
vance at neurotica.com
Thu Feb 20 21:10:32 CST 2003
On Thu, 20 Feb 2003, James Lockwood wrote:
> > Be careful about accumulation of condensate.
>
> Nitrogen or argon blanket in a glovebox, I expect. Toss in a bunch of
> Drie-Rite. Dunk in acetone to pull surface water out, any water or ice
> left will evaporate much more rapidly than straight H2O due to
> azeotrope-type behaviour at relatively low vapor pressure. Come to
> think of it, as long as you're maintaining positive pressure with
> relatively heavy CO2, moisture may not be much of a problem.
Also you have to make sure that whatever your're blowing the CO2 across
warms back up above dewpoint before you allow it to sit in room-humid air.
> A big glovebox is trivial to build compared with large precision optics.
I tend to pack bagged Na2SO4.
Peace... Sridhar
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